1297613-76-3
- Product Name：(11aR)-3,7-Bis[3,5-bis(trifluoromethyl)phenyl]-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin
- Molecular Formula：C33H19F12O4P
- Purity：99%
- Molecular Weight：738.466
Product Details
pd_meltingpoint:>300℃
Purity:99%
Best Quality Buy Reliable Quality (11aR)-3,7-Bis[3,5-bis(trifluoromethyl)phenyl]-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin 1297613-76-3 In Bulk Supply
- Molecular Formula:C33H19F12O4P
- Molecular Weight:738.466
- Melting Point:>300℃
- Boiling Point:642.3±65.0 °C(Predicted)
- PKA:1.13±0.20(Predicted)
- PSA：65.57000
- Density:1.64±0.1 g/cm3 (20 oC 760 Torr)
- LogP:11.14590
1297613-76-3 Relevant articles
Optically active 1,1′-Spirobiindane-7,7′-diol (SPINOL)-based phosphoric acids as highly enantioselective catalysts for asymmetric organocatalysis
Xing, Chun-Hui,Liao, Yuan-Xi,Ng, Jaclynn,Hu, Qiao-Sheng
, p. 4125 - 4131 (2011/07/07)
The synthesis and application of a serie...
1297613-76-3 Process route
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![(R)-6,6'-bis[3,5-bistrifluoromethylphenyl]-2,2',3,3'-4H-1,1'-spiro bis[1H-indole]-7,7'-diphenol](/upload/2024/4/d9e013d3-bdd8-442b-aa62-3540c1cd0e98.png)
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(R)-6,6'-bis[3,5-bistrifluoromethylphenyl]-2,2',3,3'-4H-1,1'-spiro bis[1H-indole]-7,7'-diphenol
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1297613-76-3,1258327-07-9
C33H19F12O4P
Conditions
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 2 steps
1: pyridine; trichlorophosphate / Inert atmosphere
2: hydrogenchloride; water; acetic acid / 1,2-dichloro-ethane / Reflux
With
pyridine; hydrogenchloride; water; acetic acid; trichlorophosphate;
In
1,2-dichloro-ethane;
|
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![(R)-6,6'-dibromo-2,2',3,3'-tetrahydro-1,1'-spirobis[1H-indole]-7,7'-diphenol](/upload/2024/4/d664dafa-a80c-4d74-8027-671ccf7d94e2.png)
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1621066-74-7,1807777-59-8
(R)-6,6'-dibromo-2,2',3,3'-tetrahydro-1,1'-spirobis[1H-indole]-7,7'-diphenol
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1297613-76-3,1258327-07-9
C33H19F12O4P
Conditions
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate / 1,4-dioxane; toluene / 105 - 110 °C / Inert atmosphere
2: pyridine; trichlorophosphate / Inert atmosphere
3: hydrogenchloride; water; acetic acid / 1,2-dichloro-ethane / Reflux
With
pyridine; hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); water; acetic acid; trichlorophosphate;
In
1,4-dioxane; 1,2-dichloro-ethane; toluene;
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1297613-76-3 Upstream products
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1621066-74-7
(R)-6,6'-dibromo-2,2',3,3'-tetrahydro-1,1'-spirobis[1H-indole]-7,7'-diphenol
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