361543-07-9
- Product Name：Azido-PEG8-azide
- Molecular Formula：
- Purity：99%
- Molecular Weight：464.519
Product Details
Purity:99%
Factory Supply High Purity Azido-PEG8-azide 361543-07-9 Safe Delivery
- Molecular Formula:C18H36N6O8
- Molecular Weight:464.519
361543-07-9 Relevant articles
Synthesis and analysis of polyethylene glycol linked P-glycoprotein-specific homodimers based on (-)-stipiamide
Andrus, Merritt B.,Turner, Timothy M.,Updegraff, Emily P.,Sauna, Zuben E.,Ambudkar, Suresh V.
, p. 3819 - 3822 (2007/10/03)
A series of five homodimeric polyethylen...
361543-07-9 Process route
-
- 3386-18-3
nonaethylene glycol
-
![1,2-bis-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethane](/upload/2024/4/bc11f557-6feb-4ff2-a39e-e5df18222a23.png)
- 361543-07-9
1,2-bis-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethane
Conditions
| Conditions | Yield |
|---|---|
|
nonaethylene glycol; With methanesulfonyl chloride; triethylamine;
With sodium azide; In ethanol;
|
95% |
-
![2,2'-[1,2-ethanediylbis(oxy)]bisethanol](/upload/2024/4/eacc551a-4270-4f50-87a4-c4486f056049.png)
- 112-27-6
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
-
- 361543-07-9
1,2-bis-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethane
Conditions
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 4 steps
1.1: 73 percent / NaOH / H2O / Heating
2.1: 73 percent / NaH / tetrahydrofuran / 20 h / Heating
3.1: 88 percent / H2 / Pd/C 10 percent / methanol / 10343 Torr
4.1: MsCl; Et3N
4.2: 95 percent / NaN3 / ethanol
With sodium hydroxide; hydrogen; sodium hydride; methanesulfonyl chloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; water;
|
|
|
Multi-step reaction with 4 steps
1.1: 97 percent / trietylamine / CH2Cl2
2.1: 73 percent / NaH / tetrahydrofuran / 20 h / Heating
3.1: 88 percent / H2 / Pd/C 10 percent / methanol / 10343 Torr
4.1: MsCl; Et3N
4.2: 95 percent / NaN3 / ethanol
With hydrogen; sodium hydride; methanesulfonyl chloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
|
361543-07-9 Upstream products
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105891-55-2
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